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Herein, we develop a protocol for the synthesis of polyimides in high yields and short reaction times of usually less than 1 h (Figure 1 ). As a model reaction the polymerization between pyromellitic dianhydride (PMDA) and 1,3,5-tri (4-aminophenyl)benzene (TAB) was chosen. Furthermore, we expanded the concept to different polymer architectures.

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2.6.1 Ball size distribution in tumbling mills 37 2.6.2 Milling performance of a ball size distribution 40 2.7 Summary 41 Chapter 3 Experimental equipment and programme 43 3.1 Laboratory grinding mill configuration 43 3.2 Preparation of mono-size grinding media 44 3.3 Feed material preparation 46 ...

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